Fabrication-free assessment of microwave losses in germanium-based dielectrics and superconductors

  1. Haoran Lu,
  2. Kushagra Aggarwal,
  3. Xiangqin Wang,
  4. Pauline Drexler,
  5. Daniel Tong,
  6. Maciej W. Olszewski,
  7. Anand Ithepalli,
  8. Lingda Kong,
  9. Debdeep Jena,
  10. Peter L. McMahon,
  11. David A. Muller,
  12. Dominique Bougeard,
  13. and Valla Fatemi
We present a flip-chip-based sensing scheme to measure effective microwave losses associated with target materials for quantum technologies, without requiring any device fabrication
on the material under test. Using this approach, we quantify the microwave losses of a strain-engineered Ge/SiGe quantum well heterostructure and investigate losses arising from its Ge substrate and intermediate layers. The quality factors of the fabricated microwave resonators agree with the losses of dielectric materials independently extracted from flip-chip sensing measurements. We further study the superconductor platinum silicon germanide (PtSiGe) prepared by thermal reaction with a deposited Pt film, finding high microwave losses that limit the suitability of the films studied here as the sole superconductor for high-quality resonator applications. By coating Pt with Nb prior to the reaction, we observe a substantial reduction in microwave loss and a nearly three-fold enhancement of the transport critical temperature. The temperature dependence of the microwave loss is consistent with gap inhomogeneity in both superconducting films. These results identify constraints on material choices, provide design guidance for microwave circuits on planar Ge heterostructures, and demonstrate a fast-turnaround testing method for new materials for superconducting quantum circuits.

High-Q superconducting microwave resonators using MBE titanium nitride

  1. Anand Ithepalli,
  2. Haoran Lu,
  3. Eegene Clara Chung,
  4. Xiangqin Wang,
  5. Amit Rohan Rajapurohita,
  6. Keun-Yeol Park,
  7. Celesta S. Chang,
  8. Peter McMahon,
  9. Huili Grace Xing,
  10. David Muller,
  11. Valla Fatemi,
  12. and Debdeep Jena
Using molecular beam epitaxy, we have realized thin films of titanium nitride (TiN) on c-plane sapphire that exhibit the lowest observed full-width at half maximum X-ray rocking curve
width of 18 arcsec. Though the (111) oriented TiN exhibits an abrupt and crystalline interface with sapphire, for the first time we observe sub-surface defects in the sapphire substrate, which nucleate structural defects in the epitaxial TiN layer. Using quarter-wavelength coplanar waveguide (CPW) resonators in a 3 \textmu m/6 \textmu m/3 \textmu m gap/strip/gap lines in a hanger geometry, we find the internal quality factor of the TiN resonators to be >106 in the single-photon ⟨n⟩∼1 limit at 5.8 GHz and 10 mK, rising to >20×106 at ⟨n⟩∼106. The results are of high interest for applications of superconducting TiN in several areas, and provide a path towards epitaxial Josephson junctions with crystalline barriers in the future for high coherence qubits.

Krypton-sputtered tantalum films for scalable high-performance quantum devices

  1. Maciej W. Olszewski,
  2. Lingda Kong,
  3. Simon Reinhardt,
  4. Daniel Tong,
  5. Xinyi Du,
  6. Gabriele Di Gianluca,
  7. Haoran Lu,
  8. Saswata Roy,
  9. Luojia Zhang,
  10. Aleksandra B. Biedron,
  11. David A. Muller,
  12. and Valla Fatemi
Superconducting qubits based on tantalum (Ta) thin films have demonstrated the highest-performing microwave resonators and qubits. This makes Ta an attractive material for superconducting
quantum computing applications, but, so far, direct deposition has largely relied on high substrate temperatures exceeding \SI{400}{\celsius} to achieve the body-centered cubic phase, BCC (\textalpha-Ta). This leads to compatibility issues for scalable fabrication leveraging standard semiconductor fabrication lines. Here, we show that changing the sputter gas from argon (Ar) to krypton (Kr) promotes BCC Ta synthesis on silicon (Si) at temperatures as low as \SI{200}{\celsius}, providing a wide process window compatible with back-end-of-the-line fabrication standards. Furthermore, we find these films to have substantially higher electronic conductivity, consistent with clean-limit superconductivity. We validated the microwave performance through coplanar waveguide resonator measurements, finding that films deposited at \SI{250}{\celsius} and \SI{350}{\celsius} exhibit a tight performance distribution at the state of the art. Higher temperature-grown films exhibit higher losses, in correlation with the degree of Ta/Si intermixing revealed by cross-sectional transmission electron microscopy. Finally, with these films, we demonstrate transmon qubits with a relatively compact, \SI{20}{\micro\meter} capacitor gap, achieving a median quality factor up to 14 million.

Low-loss Nb on Si superconducting resonators from a dual-use spintronics deposition chamber and with acid-free post-processing

  1. Maciej W. Olszewski,
  2. Jadrien T. Paustian,
  3. Tathagata Banerjee,
  4. Haoran Lu,
  5. Jorge L. Ramirez,
  6. Nhi Nguyen,
  7. Kiichi Okubo,
  8. Rohit Pant,
  9. Aleksandra B. Biedron,
  10. Daniel C. Ralph,
  11. Christopher J. K. Richardson,
  12. Gregory D. Fuchs,
  13. Corey Rae H McRae,
  14. Ivan V. Pechenezhskiy,
  15. B. L. T. Plourde,
  16. and Valla Fatemi
Magnetic impurities are known to degrade superconductivity. For this reason, physical vapor deposition chambers that have previously been used for magnetic materials have generally
been avoided for making high-quality superconducting resonator devices. In this article, we show by example that such chambers can be used: with Nb films sputtered in a chamber that continues to be used for magnetic materials, we demonstrate compact (3 {\mu}m gap) coplanar waveguide resonators with low-power internal quality factors near one million. We achieve this using a resist strip bath with no post-fabrication acid treatment, which results in performance comparable to previous strip baths with acid treatments. We also find evidence that this improved resist strip bath provides a better surface chemical template for post-fabrication hydrogen fluoride processing. These results are consistent across three Si substrate preparation methods, including a \SI{700}{\celsius} anneal.